Aerogel Recipes

Procedures for making aerogels of various types.

Nickel Oxide Aerogels

Lawrence Livermore synthesis of pastel green nickel oxide aerogels using epoxide-assisted gelation.

Zinc Oxide Aerogels

The synthesis of white, monolithic ZnO aerogels developed by Prof. Louisa Hope-Weeks at Texas Tech University.

Organic Aerogels

The synthesis of organic aerogels (of resorcinol-formaldehyde polymer, to be exact) based on the work of Dr. Rick Pekala and co-workers at Lawrence Livermore. They are cranberry-sauce red and are suitable precursors to carbon aerogels. Use the Pyrolysis procedure to make carbon aerogels from them.

Alumina Aerogels (Epoxide-Assisted)

Lawrence Livermore synthesis of transparent, high-quality alumina aerogels using epoxide-assisted gelation.

Alumina Aerogels (Alkoxide Method)

Synthesis of high-porosity, high-strength alumina aerogels using an aluminum alkoxide.

Silica Aerogel (TEOS, Base-Catalyzed)

Classic base-catalyzed TEOS procedure for producing transparent silica aerogels.

Iron Oxide Aerogels

Rigid, rust-colored iron oxide aerogels made by epoxide-assisted gelation. Favorite aerogel of Dr. Alex Gash!

Silica Aerogel (TMOS, Base-Catalyzed)

Nice, base-catalyzed TMOS procedure for preparing transparent silica aerogels suitable for optical analysis (recipe contributed by Michael Grogan, University of Bath, UK). Same recipe presented in our podcast Episode 5.

Pyrolysis

Procedure for producing carbon aerogels and other derivative aerogels prepared by heat-treating aerogel precursors.

Hydrophobic and Subcritically-Dried Silica Aerogel

Procedure for preparing waterproof silica aerogels. Can be prepared with supercritical or subcritical drying. Includes process for subcritical drying.